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HEROIN SYNTHESIS FROM MORPHINE
* Thread starter G.Patton
* Start date Jul 28, 2023
* Tags acetic anhydride heroin morphine synthesis
G.PATTON
Expert
Joined Jul 5, 2021 Messages 2,354 Solutions 3 Reaction score 2,264 Points 113
Deals 1
* Jul 28, 2023
*
* #1
INTRODUCTION
The key chemical used in the acetylation of morphine to form heroin is acetic
anhydride, a colorless, highly combustible liquid with a strong pickle-like
odor. Though internationally controlled as a heroin precursor, acetic anhydride
also used to synthesize aspirin and chemicals for leather tanning and
photography.
MORPHINE CONVERSION TO HEROIN BASE
1. Morphine hydrochloride or morphine base is mixed with acetic anhydride (Ac2O)
at about three-times the mass of the former in a glass, stainless steel or
enamel pot.
2. The pot lid is tied or clamped on with a damp towel for a gasket (a makeshift
reflux apparatus), and the mixture is heated at 85 °C (185 °F), avoiding
boiling.
Note: you can use glass reactor with reflux condenser.
3. The reaction is heated for about 5 h until all the morphine has dissolved.
4. The pot is opened, and the mixture is a solution of water, acetic acid, and
diacetylmorphine (heroin), is cooled to a room temperature.
5. Water is added to the mixture at three-times the volume of acetic anhydride,
and the mixture is stirred.
6. A small amount of chloroform is added. The mixture is allowed to stand for 20
min. The chloroform dissolves colored impurities and settles to the bottom of
the pot as a red, greasy liquid, and the water layer is carefully poured off.
7. Activated charcoal is added to the mixture (chloroform solution), absorbing
solid impurities, which are filtered out repeatedly until the solution is clear.
8. Approximately 2.2 kg of sodium carbonate (soda ash) per kg of morphine are
dissolved in hot water, added slowly to the mixture until effervescence stops,
precipitating solid heroin base.
9. Heroin base is dried. The heroin base should be a granular, white powder at
this point. If still colored (beige or light brown), the base may be
re-dissolved in dilute hydrochloric or citric acid, treated with charcoal again,
re-precipitated and dried.
10. Alternatively, in some manufacturing regions, the incompletely purified base
may be packed and transported for sale (a practice probably typical in Southwest
Asia). About 700 g of heroin base will be produced from each kg of morphine.
ADDITIONAL PURIFICATION
Optionally, skilled heroin chemists may further purify the base by dissolving it
in twice its mass of boiling ethyl alcohol, filtering the solution through a
heated funnel into a heated flask. This removes traces of sodium carbonate
remaining in the base. The flask is submerged in an ice bath, where it is
transformed into a thick white cream. The substance is placed in a pan in a
refrigerator with a fan set to blow across the pan to slowly evaporate the
alcohol. The paste crystallizes after several hours and is then vacuum filtered.
The product, referred to as alcohol morphine base, is re-crystallized heroin
base.
CONVERSION OF HEROIN BASE TO HEROIN HYDROCHLORIDE
1. For each kilogram of heroin base (or re-crystallized heroin base), 6.6 L of
of ethyl alcohol, 6.6 L of diethyl ether, and 225 mL of concentrated
hydrochloric acid are measured out. The base is dissolved by heating with
one-third of the alcohol and one half of the acid.
2. Another one-third of the acid is stirred in. Next, the remaining acid is
added slowly, dropwise, until the product is completely converted to the
hydrochloride salt. This result may be confirmed either by observing that a drop
of solution evaporates on a glass plate leaving no cloudy residue or by placing
a drop of solution on Congo red paper, observing it turn the paper blue.
3. Once the conversion is complete, the remaining alcohol is stirred in. Then
half of the ether is added, and the mixture is allowed to stand for 15 min.
4. As soon as crystals begin to form in the solution, the remaining ether is
added at once, stirred, and the the vessel is covered. The mixture becomes
nearly solid after an hour.
5. It is then filtered, and the solids are collected on clean filter paper.
Wrapped in the paper, the solid is dried on a wooden tray, usually over lime
rock, and dried in a desiccator (optionally). The fully dried product, heroin
hydrochloride, is a fine white powder, ready for packing and shipping.
Last edited: Jul 28, 2023
*
Reactions: Emelia, nkd23, HEISENBERG and 1 other person
N
NKD23
DON'T BUY FROM ME
Resident
Joined Nov 18, 2022 Messages 22 Reaction score 5 Points 3
* 28 Jul
*
* #2
Yeah thank you!
Ia it possible too downscale the synthese? (10-50g morphine)
The makeshift glass reactor could be a round bottom flask with an allhine
condenser on top with a cacl filled drIngtube?
If the morphine is extracted from tablets is it possible that I don't need the
to chlorophorm step?
Thank a lot!
DERBRATLING
DON'T BUY FROM ME
New Member
Joined Jan 31, 2024 Messages 3 Reaction score 0 Points 1
* By DerBratling
* 31 Jan
*
* #12
> nkd23 said:
> Yeah thank you!
>
> Ia it possible too downscale the synthese? (10-50g morphine)
>
> The makeshift glass reactor could be a round bottom flask with an allhine
> condenser on top with a cacl filled drIngtube?
>
> If the morphine is extracted from tablets is it possible that I don't need the
> to chlorophorm step?
>
>
> Thank a lot!
> Click to expand...
nkd23@nkd23
Your makeshift glass reactor sounds good, but boiling that stuff 5h is not the
smartest option. Better use a catalyst as descriebed in the following synthesis:
> In a 10 ml centrifuge tube, 28.5 mg morphine, 29.4 mg
> N,N-(dimethylamino)-pyridine, 1 ml dichloromethane (DCM) and 100 µ l acetic
> anhydride are added. The mixture is left to stand for 5 to 6 min. After the
> time has elapsed, 2 ml water is added to the mixture and shaken out in a
> separating funnel with 10 ml dichloromethane. The water is separated off and
> the organic phase is dried with anhydrous sodium sulphate. After evaporation
> of the solvent, heroin remains.
> Click to expand...
But the pretty hard shit is to purify the morphine from tablets. But I've
already written enough about that below.
N
NKD23
DON'T BUY FROM ME
Resident
Joined Nov 18, 2022 Messages 22 Reaction score 5 Points 3
* 28 Jul
*
* #3
And the finished product is good for nasal or smoking?
ZIPPY53
DON'T BUY FROM ME
Resident
Joined Feb 17, 2023 Messages 10 Reaction score 20 Points 3
* 29 Jul
*
* #4
Hello again...Since you did such a nice write up of Black tar opium extraction
from poppy plant material and now this recipe for heroin, it would be great if
you had time to fill in the middle part...
Meaning, for example, taking the product produced from your BTO recipe, then
converting that into the morphine hcl one would need to produce the
heroin...Seems to be hard to find a proven method for this when starting with a
small amount of opium...I have a few grams of opium to play around with so I
will try a scaled down version of the Afghani process as an experiment..
Anyways, if you have any input that would be great.
*
Reactions: nkd23
DERBRATLING
DON'T BUY FROM ME
New Member
Joined Jan 31, 2024 Messages 3 Reaction score 0 Points 1
* By DerBratling
* 31 Jan
*
* #11
> Zippy53 said:
> Hello again...Since you did such a nice write up of Black tar opium extraction
> from poppy plant material and now this recipe for heroin, it would be great if
> you had time to fill in the middle part...
> Meaning, for example, taking the product produced from your BTO recipe, then
> converting that into the morphine hcl one would need to produce the
> heroin...Seems to be hard to find a proven method for this when starting with
> a small amount of opium...I have a few grams of opium to play around with so I
> will try a scaled down version of the Afghani process as an experiment..
> Anyways, if you have any input that would be great.
> Click to expand...
Zippy53
> Meaning, for example, taking the product produced from your BTO recipe, then
> converting that into the morphine hcl one would need to produce the heroin.
> Click to expand...
This sounds very tempting, but tablets such as Substitol are very difficult to
extract in an acceptable purity. They contain polymers and soaps that swell the
powder into a viscous mass on contact with water and have horrible
physicochemical properties.
Such a slurry is not suitable for diacetylation to heroin.
However, there are various methods that describe the extraction of ephedrine
from tablets. The one with activated charcoal and starch could also work with
Substitol.
D
DEPOT1223
DON'T BUY FROM ME
Member
Joined Sep 1, 2023 Messages 2 Reaction score 0 Points 1
* 07 Sep
*
* #5
This is stolen from erowid post was made by a guy named samson. I asked a basic
question and the guy had no clue what he was talking about.
41DXFLATLINE
DON'T BUY FROM ME
Resident
Joined Dec 23, 2022 Messages 326 Solutions 1 Reaction score 138 Points 43
* By 41Dxflatline
* 07 Sep
*
* #6
> depot1223 said:
> This is stolen from erowid post was made by a guy named samson. I asked a
> basic question and the guy had no clue what he was talking about.
> Click to expand...
depot1223G. Patton knows what he's talking about. It doesn't matter where he got
the procedure from because whoever posted it to Erowid certainly didn't invent
it and copied it from somewhere else.
D
DEPOT1223
DON'T BUY FROM ME
Member
Joined Sep 1, 2023 Messages 2 Reaction score 0 Points 1
* By depot1223
* 08 Sep
*
* #7
> 41Dxflatline said:
> G. Patton knows what he's talking about. It doesn't matter where he got the
> procedure from because whoever posted it to Erowid certainly didn't invent it
> and copied it from somewhere else.
> Click to expand...
41DxflatlineThe write up is copied and slightly paraphrased. I know. I doubt he
knows about this specific synth. I asked if the #3 to #4 conversion scales down,
and how much heat it should take to dissolve. Got the run around. Pretty much
refused to answer.
J
JOTAS
DON'T BUY FROM ME
Member
Joined Dec 1, 2023 Messages 2 Reaction score 0 Points 1
* 12 Dec
*
* #8
Hello, good. Very good link, thank you! I wanted to know if starting from
morphine sulphate I have to transform it into chlorine hydrate.? Is the passage
of chloroform necessary?
G
GMO
DON'T BUY FROM ME
Resident
Joined Feb 25, 2023 Messages 25 Reaction score 2 Points 3
* 21 Jan
*
* #9
> G.Patton said:
> View attachment 19402
> INTRODUCTION
>
> The key chemical used in the acetylation of morphine to form heroin is acetic
> anhydride, a colorless, highly combustible liquid with a strong pickle-like
> odor. Though internationally controlled as a heroin precursor, acetic
> anhydride also used to synthesize aspirin and chemicals for leather tanning
> and photography.
> View attachment 19404
> MORPHINE CONVERSION TO HEROIN BASE
>
> 1. Morphine hydrochloride or morphine base is mixed with acetic anhydride
> (Ac2O) at about three-times the mass of the former in a glass, stainless steel
> or enamel pot.
>
> 2. The pot lid is tied or clamped on with a damp towel for a gasket (a
> makeshift reflux apparatus), and the mixture is heated at 85 °C (185 °F),
> avoiding boiling.
> Note: you can use glass reactor with reflux condenser.
>
> 3. The reaction is heated for about 5 h until all the morphine has dissolved.
>
> 4. The pot is opened, and the mixture is a solution of water, acetic acid, and
> diacetylmorphine (heroin), is cooled to a room temperature.
>
> 5. Water is added to the mixture at three-times the volume of acetic
> anhydride, and the mixture is stirred.
>
> 6. A small amount of chloroform is added. The mixture is allowed to stand for
> 20 min. The chloroform dissolves colored impurities and settles to the bottom
> of the pot as a red, greasy liquid, and the water layer is carefully poured
> off.
>
> 7. Activated charcoal is added to the mixture (chloroform solution), absorbing
> solid impurities, which are filtered out repeatedly until the solution is
> clear.
>
> 8. Approximately 2.2 kg of sodium carbonate (soda ash) per kg of morphine are
> dissolved in hot water, added slowly to the mixture until effervescence stops,
> precipitating solid heroin base.
>
> 9. Heroin base is dried. The heroin base should be a granular, white powder at
> this point. If still colored (beige or light brown), the base may be
> re-dissolved in dilute hydrochloric or citric acid, treated with charcoal
> again, re-precipitated and dried.
>
> 10. Alternatively, in some manufacturing regions, the incompletely purified
> base may be packed and transported for sale (a practice probably typical in
> Southwest Asia). About 700 g of heroin base will be produced from each kg of
> morphine.
>
> ADDITIONAL PURIFICATION
>
> در صورت تمایل، شیمیدانان ماهر هروئین ممکن است پایه را با حل کردن آن در دو
> برابر جرم آن از الکل اتیل در حال جوش، خالص سازی بیشتری انجام دهند و محلول را
> از طریق یک قیف گرم شده در یک فلاسک گرم شده فیلتر کنند. این کار باعث حذف آثار
> کربنات سدیم باقی مانده در پایه می شود. فلاسک در یک حمام یخ غوطه ور می شود و در
> آنجا به یک کرم سفید غلیظ تبدیل می شود. این ماده را در یک تابه در یخچال قرار
> میدهیم که یک فن در آن قرار میگیرد تا به آرامی الکل تبخیر شود. خمیر پس از چند
> ساعت متبلور می شود و سپس با خلاء فیلتر می شود. این محصول که به عنوان پایه
> مورفین الکل شناخته می شود، پایه هروئینی متبلور مجدد است.
> View attachment 19403
> تبدیل پایه هروئین به هروئین هیدروکلراید
>
> 1. برای هر کیلوگرم پایه هروئین (یا باز کریستالی شده هروئین)، 6.6 لیتر اتیل
> الکل، 6.6 لیتر دی اتیل اتر، و 225 میلی لیتر اسید هیدروکلریک غلیظ اندازه گیری
> می شود. پایه با حرارت دادن با یک سوم الکل و نیمی از اسید حل می شود.
>
> 2. یک سوم دیگر اسید هم زده می شود. سپس اسید باقیمانده به آرامی و به صورت قطره
> ای اضافه می شود تا محصول کاملاً به نمک هیدروکلراید تبدیل شود. این نتیجه ممکن
> است با مشاهده اینکه یک قطره از محلول روی یک صفحه شیشه ای تبخیر می شود و هیچ
> باقیمانده ای کدر نمی کند یا با قرار دادن یک قطره محلول روی کاغذ قرمز کنگو و
> مشاهده اینکه کاغذ را آبی می کند تأیید می شود.
>
> 3. هنگامی که تبدیل کامل شد، الکل باقیمانده به هم زده می شود. سپس نیمی از اتر
> اضافه می شود و مخلوط به مدت 15 دقیقه باقی می ماند.
>
> 4. به محض اینکه کریستال ها در محلول تشکیل شدند، اتر باقیمانده را یکباره اضافه
> می کنند، هم می زنند و ظرف را می پوشانند. مخلوط پس از یک ساعت تقریباً جامد می
> شود.
>
> 5. سپس فیلتر می شود و مواد جامد روی کاغذ صافی تمیز جمع آوری می شوند. جامد که
> در کاغذ پیچیده می شود، روی یک سینی چوبی، معمولاً روی سنگ آهک، خشک می شود و در
> یک خشک کن (اختیاری) خشک می شود. محصول کاملاً خشک شده هروئین هیدروکلراید یک
> پودر سفید ریز است که آماده بسته بندی و حمل است.
> Click to expand...
G.Pattonمنdon't want use ether just alcohol it's ok?
G.PATTON
Expert
Joined Jul 5, 2021 Messages 2,354 Solutions 3 Reaction score 2,264 Points 113
Deals 1
* By G.Patton
* 21 Jan
*
* #10
> gmo said:
> منdon't want use ether just alcohol it's ok?
> Click to expand...
gmonot ok
N
NKD23
DON'T BUY FROM ME
Resident
Joined Nov 18, 2022 Messages 22 Reaction score 5 Points 3
* 25 Feb
*
* #13
7. Activated charcoal is added to the mixture (chloroform solution), absorbing
solid impurities, which are filtered out repeatedly until the solution is clear
do I work with the chloroform part or the water layer?
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