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Submission: On March 20 via manual from US — Scanned from DE
Submission: On March 20 via manual from US — Scanned from DE
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<h2 class="AuthorHeader-module__syvlN margin-size-4-t">El-Bahy, Zeinhom Mohamed A.</h2><input type="hidden" name="authorPreferredName" class="hidden" value="El-Bahy, Zeinhom Mohamed A.">
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</els-tooltip><span class=""><a href="https://www.scopus.com/affil/profile.uri?afid=60004871" class="disabled" style="display: inline;"><span class="link__text">Al-Azhar University</span><span class="sr-only">disabled</span></a>,
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<h4 class="margin-size-20-b">Most contributed Topics 2016–2020<span><els-popout targetelementid="info-button-area-of-expertise" position="above-left" id="info-popout" open="false">
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<div class="list-title margin-size-24-t margin-size-0-b text-width-32"><els-typography tag="h4" variant="documents-title" bold="false" family="sans" size="xs" class="hydrated"><span class="list-title">Electronic
structure, optical, thermoelectric and magnetic properties of A<sub>2</sub>CdP<sub>2</sub> (A = Ca, Sr and Ba) n-type narrow band gap semiconductors</span></els-typography></div>
<div data-component="document-authors" class="author-list"><span><els-button variant="link" size="s" href="/authid/detail.uri?authorId=55781587300" tabindex="0" class="hydrated">Aman, S.</els-button></span>,
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<div class="text-width-38">Structural, Optoelectronic, thermoelectric and magnetic properties of A2CdP2 (A = Ca, Sr and Ba) Zentl phase compounds in Cmc21 symmetry are investigated using FP-LAPW method with
GGA-PBE, GGA-PBEsol, HSE06, G0W0 and GGA-mBJ potentials based on DFT. Estimated structure parameters are well agreement with the experiment. Cohesive energy shows that Ba2CdP2 is more stale then the rest
compounds and posses high melting point. Electronic properties shows that all the compounds are direct band gap semiconductors at central symmetry while GGA-mBJ transit the direct band gap nature to
indirect nature at ᴦ-H symmetry. The direct band gap values are ranging from 0.74 to 1.47 eV. The calculated band gaps are decreasing with the cation replacement and increasing by hybrid functionals. The
result revel that all the compounds are optically active in infrared region of electromagnetic spectrum. Optical properties reveals that these compounds can be used as potential candidate for
optoelectronic devices. Due to the narrow band gap semiconducting nature of these compounds their thermoelectric parameters are also calculated which shows that these compounds are efficient to use as the
active thermoelectric materials. DFT and Post-DFT calculation indicate the paramagnetic nature of all compounds.</div>
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dispersed active sites of Ni nanoparticles onto hierarchical reduced graphene oxide architecture towards efficient water oxidation</span></els-typography></div>
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<div class="text-width-38">Herein, we reported a facile route to fabricate the Ni-NPs decorated over reduced graphene oxide (Ni/rGO) nanocomposite by an in-situ reduction method. It has been observed that
the Ni/rGO drived the water oxidation at a very low overpotential of 1.42 VRHE (ŋ = 190 mV). Furthermore, the robust catalyst presented an extraordinary porosity and imperious kinetics performance while
showing a high time of flight (0.2 s−1), mass activity (28 A/g) and smaller value of Tafel slope (62 mVdec−1) at an applied potential of 0.35 VRHE only. Ni/rGO also exhibited stable current density which
leftovers sustained in alkaline water catalysis conducted for a prolonged time without any significant loss in catalytic efficiency. This outstanding catalytic activity of hierarchical Ni/rGO is
comparable to avant-garde electrocatalytic material and even much better than the noble and transitional metal-centred eensy-weensy electrocatalytic assemblies with several drawbacks.</div>
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OLi<sub>3</sub> and MgF<sub>3</sub> doped boron nitride with enhanced nonlinear optical behavior</span></els-typography></div>
<div data-component="document-authors" class="author-list"><span><els-button variant="link" size="s" href="/authid/detail.uri?authorId=57357742100" tabindex="0" class="hydrated">Shafiq, S.</els-button></span>,
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<a href="#disabled" title="Show document details" class="source-link disabled" tabindex="-1" data-publisher="Elsevier B.V."><span class="link__text text-meta text-bold text-italic">Journal of Molecular Structure</span><span class="sr-only">this link is disabled</span></a>,
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<div class="text-width-38">The electrical and optical properties of superalkali (OLi3) and superhalogen (MgF3) doped boron nitride nanocage are investigated. Superalkali and superhalogen are doped
physically and substitutionally with boron nitride and its geometrical and optoelectronic properties are analyzed and compared systematically. In the doped nanocage of boron nitride, the linear optical
polarizability and nonlinear optical hyperpolarizability increases to a greater extent. The increasing trend of the hyperpolarizability in the nanocage of metal-doped boron nitride depends on the
atomicity of superhalogen and superalkali metal. The energy bandgap of HOMO-LUMO also decreases due to the injection of new energy levels in all the doped compounds of boron nitride near the Fermi level.
Among different combinations, MgF3 and OLi3 doped with B12N10 found the most reliable combination with enhanced linear and nonlinear optical polarizability. The current clue gives wide applications for
boron nitride nanocage in electrical instruments and devices that play an important role in the designing of efficient nonlinear optical materials.</div>
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silico and in vitro studies of Silver (I)-N heterocyclic carbene complexes</span></els-typography></div>
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<div class="text-width-38">In the present study, four silver based NHC (N-heterocyclic carbene) complexes (1c-4c) were designed and synthesized from their precursor salts (1b-4b). The successful synthesis
of salts and complexes was assured through spectroscopic techniques (UV-visible, FTIR, 1H NMR) as well as mass spectrometry. The in silico ADMET study and molecular docking calculations predicted the
compounds are good drug candidates having therapeutic potential against multiple cancer targets including COX-1, VEGFA, HIF as well as VGF. Results of in vitro study conducted through MTT assay confirmed
that all test compounds have concentration dependent potency but silver complexes (1c-4c) have far superior activity than precursor, salts (1b-4b) and slightly lower than standard drugs (carboplatin and
cisplatin) against various cancer cell lines. Among the studied compounds, 3c showed lowest IC50 value of 0.981 ± 0.09, 1.10 ± 0.14 and 0.973 ± 0.12 µg/mL against MCF-7, HCT-116 and A549 respectively. The
test compounds were found good antibacterial agents, when screened against bacterial strains (Staphylococcus aureus, Micrococcus luteus, Escherichia coli and S. typhimurium), as well as antioxidant agents
when tested against DPPH free radicals.</div>
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crystallized using novel pyridinium template as highly active catalyst for synthesis of ethyl levulinate biofuel</span></els-typography></div>
<div data-component="document-authors" class="author-list"><span><els-button variant="link" size="s" href="/authid/detail.uri?authorId=57219379935" tabindex="0" class="hydrated">Ma, Y.-K.</els-button></span>,
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<a href="#disabled" title="Show document details" class="source-link disabled" tabindex="-1" data-publisher="Elsevier B.V."><span class="link__text text-meta text-bold text-italic">Microporous and Mesoporous Materials</span><span class="sr-only">this link is disabled</span></a>,
<span class="text-meta">2022, 333, 111754</span></div><els-collapsible-panel-v2 open="false" data-testid="document-abstract-link" data-component="document-abstract-link" control-label="Show abstract"
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<div class="text-width-38">Silicoaluminophosphate Number 34 (SAPO-34) crystallized using novel N-heterocyclic organic template—1-propylpyridinium hydroxide ([PPy]OH)—as an excellent catalyst for the
production of ethyl levulinate biofuel is reported. First, the time-dependent crystallization study of SAPO-34 using various spectroscopy, microscopy and analytical techniques is performed and it reveals
that the precursor undergoes several important crystallization steps, namely dissolution of reactants (induction), nucleation and crystal growth of SAPO-34, before it transforms into a more metastable
SAPO-36 crystalline phase. The resulting SAPO-34 solid (Si0.198Al0.475P0.327O2) exhibits high porosity (SBET = 673 m2/g, VTot = 0.27 cm3/g) and high Si content (Si/(Si + Al + P) = 0.198) which contribute
to high surface acidity (2.52 mmol/g) as confirmed by the NH3-TPD analysis. The SAPO-34 catalyst shows 93.4% conversion to ethyl levulinate via esterification of levulinic acid with ethanol just within 20
min at 190 °C under non-microwave instant heating, which is considered very fast as compared to other systems. In addition, high catalyst recyclability is observed even after fifth cycle of reaction, thus
offering another promising pathway for crystallizing zeolites using this new class of template that are beneficial for catalytic biofuel upgrading process.</div>
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<div class="list-title margin-size-24-t margin-size-0-b text-width-32"><els-typography tag="h4" variant="documents-title" bold="false" family="sans" size="xs" class="hydrated"><span class="list-title">ZIF-8-derived
ZnO/C decorated hydroxyl-functionalized multi-walled carbon nanotubes as a new composite electrode for supercapacitor application</span></els-typography></div>
<div data-component="document-authors" class="author-list"><span><els-button variant="link" size="s" href="/authid/detail.uri?authorId=56939031300" tabindex="0" class="hydrated">Otun, K.O.</els-button></span>,
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href="/authid/detail.uri?authorId=55235107300" tabindex="0" class="hydrated">Zong, S.</els-button></span>, ...<span><els-button variant="link" size="s" href="/authid/detail.uri?authorId=57194192844"
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Z.M.</els-button></span></div>
<div data-component="document-source" class="text-meta text-width-34"><span class="text-bold text-italic">Colloids and Interface Science Communications</span>, <span class="text-meta">2022, 47, 100589</span></div>
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<div class="text-width-38">Due to the poor conductivity of metal-organic frameworks (MOFs), it is challenging to directly employ MOFs as electrode materials for supercapacitors. Herein,
hydroxyl-functionalized multi-walled carbon nanotube (f-MWCNT) was used to decorate ZnO/C obtained from the prior calcination of pristine zeolitic imidazolate framework-8 (ZIF-8) and applied as electrode
material for supercapacitor application. The resulting ZnO/C@f-MWCNT electrode exhibits excellent storage performance, as confirmed by the specific capacitance of 650 F/g at 1 A/g and a superior
energy/power density compared to the single electrode. Additionally, the composite electrode displayed remarkable cycling stability of 70% after 5000 cycles and retained 75% of its initial capacitance at
10 A/g, demonstrating good rate cyclability. The exceptional performance of ZnO/C@f-MWCNT was attributed to the synergistic effects offered by f-MWCNT which improved its electrical conductivity and ZnO/C
that provided sufficient redox-active sites and structural stability. This work may promote the design of advanced MOF-based nanocomposites for energy storage application.</div>
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<div class="list-title margin-size-24-t margin-size-0-b text-width-32"><els-typography tag="h4" variant="documents-title" bold="false" family="sans" size="xs" class="hydrated"><span class="list-title">A n-butanol
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<div data-component="document-authors" class="author-list"><span><els-button variant="link" size="s" href="/authid/detail.uri?authorId=55503533700" tabindex="0" class="hydrated">Guo, W.</els-button></span>,
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<a href="#disabled" title="Show document details" class="source-link disabled" tabindex="-1" data-publisher="Elsevier B.V."><span class="link__text text-meta text-bold text-italic">Sensors and Actuators B: Chemical</span><span class="sr-only">this link is disabled</span></a>,
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<div class="text-width-38">N-butanol, a poisonous and flammable liquid, has great threat to human life and property security, which is of importance to monitor n-butanol in the environment. In this paper,
the pure and Co-doped BiVO4 polyhedrons are successfully synthesized by hydrothermal method. A series of characterizations, such as XRD, XPS, SEM, UV, and EIS, etc., are used to analyze the crystal
structure, morphology, element compositions, optical and electrochemical properties of the as-prepared samples. The optimal sample (3Co-BiVO4) exhibits high gas response (51.65) toward 100 ppm n-butanol,
which is around four times higher than that of pure BiVO4 at 300 °C. In addition, the 3Co-BiVO4 also has fast response-recovery time, good humidity resistance, favorable selectivity to n-butanol, etc.
Based on the above characterizations and gas sensing test results, the enhanced gas sensing mechanism for 3Co-BiVO4 is proposed. This work provides a feasible strategy to fabricate BiVO4 polyhedron by
doping Co to greatly enhance the gas sensing properties for n-butanol.</div>
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synthesis from Prunus bokhariensis non-edible seed oil by using green silver oxide nanocatalyst</span></els-typography></div>
<div data-component="document-authors" class="author-list"><span><els-button variant="link" size="s" href="/authid/detail.uri?authorId=57200700053" tabindex="0" class="hydrated">Dawood, S.</els-button></span>,
<span><els-button variant="link" size="s" href="/authid/detail.uri?authorId=56430353500" tabindex="0" class="hydrated">Ahmad, M.</els-button></span>, <span><els-button variant="link" size="s"
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<div class="text-width-38">The present work investigates the proficiency of green silver oxide nanocatalyst synthesised from Monotheca buxifolia (Falc.) Dcne. leaves extract, and their application for
biodiesel synthesis from novel Prunus bokhariensis seed oil (non-edible). The seed oil content of 55% and FFA content of 0.80 mg KOH/g were reported. Several analytical tools (EDX, FT-IR, SEM and XRD)
were used to characterise the Ag2O nanocatalyst. Maximum (89%) FAME yield of the PBSOB (Prunus bokhariensis seed oil biodiesel) was achieved at ambient transesterification conditions i.e. 3.5 wt%
nanocatalyst loading, 2.5 h reaction time, 130 °C of reaction temperature and 12:1 alcohol to oil ratio. The synthesised PBSOB was additionally characterised by analytical methods like, GC-MS and FT-IR.
The different aspects of fuel were identified i.e. flash point (84 °C), kinematic viscosity (4.01 cSt @ 40 °C), sulphur content (0.0003 wt %), density (0.853 kg/L) and acid number (0.167 mg KOH/g). All
the above properties were verified and agreed well with biodiesel international standards (European Union (14214), China GB/T (20828) and ASTM (6751, 951). In general, Prunus bokhariensis seed oil and
Ag2O nanocatalyst seem to be remarkably active, cheap and stable candidates for the biodiesel industry in future.</div>
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MOF-derived NiO and NiO/Ni supercapacitor electrodes for enhanced energy storage</span></els-typography></div>
<div data-component="document-authors" class="author-list"><span><els-button variant="link" size="s" href="/authid/detail.uri?authorId=56939031300" tabindex="0" class="hydrated">Otun, K.O.</els-button></span>,
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<a href="#disabled" title="Show document details" class="source-link disabled" tabindex="-1" data-publisher="Elsevier B.V."><span class="link__text text-meta text-bold text-italic">Colloids and Surfaces A: Physicochemical and Engineering Aspects</span><span class="sr-only">this link is disabled</span></a>,
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<div class="text-width-38">Metal-organic frameworks (MOFs)-derived nanomaterials have emerged as novel electrodes for electrochemical energy storage application. Herein, MOF-derived NiO and NiO/Ni composite
electrodes have been successfully synthesized by a unique double-linker MOF-strategy involving a series of calcination procedures (400 °C, 500 °C and 600 °C). The introduction of calcination temperature
influenced both the textural and electrochemical properties of the MOF-derived NiO/Ni-400 and NiO/Ni-500 composite electrodes obtained at 400 °C and 500 °C respectively, as well as the NiO-600 electrode
produced at 600 °C. With the combined benefits of improved uniform pore-size distribution and electrical conductivity, the composite electrodes delivered an enhanced supercapacitor performance with
specific capacitances of 104.6 mAg−1 (NiO/Ni-400) and 37.4 mAg−1 (NiO/Ni-500) compared with 28.5 mAg−1 for the NiO-600 electrode at the same current density. Interestingly, NiO/Ni retained about 90% of
its original capacitance after 1000 cycles when measured in 3 M KOH electrolyte solution. Furthermore, the electrochemical kinetic analysis used to probe the energy storage mechanism revealed
pseudocapacitive behaviors at all tested scan rates; with NiO/Ni contributing 67% of the total capacitance at a scan rate of 5 mV/s which increased to 87% at 100 mV/s. The results obtained confirm that
the approach described in this study is promising for the design of MOF-based electrodes for energy storage applications.</div>
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class="list-title">Ruthenium-Doping-Induced Amorphization of VS<sub>4</sub>Nanostructures with a Rich Sulfur Vacancy for Enhanced Hydrogen Evolution Reaction in a Neutral Electrolyte
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<div data-component="document-authors" class="author-list"><span><els-button variant="link" size="s" href="/authid/detail.uri?authorId=57212572233" tabindex="0" class="hydrated">Karmakar, A.</els-button></span>,
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href="/authid/detail.uri?authorId=57211622742" tabindex="0" class="hydrated">Kumaravel, S.</els-button></span>, ...<span><els-button variant="link" size="s" href="/authid/detail.uri?authorId=6506690176"
tabindex="0" class="hydrated">El-Bahy, Z.M.</els-button></span>, <span><els-button variant="link" size="s" href="/authid/detail.uri?authorId=57204293164" tabindex="0" class="hydrated">Kundu,
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<a href="#disabled" title="Show document details" class="source-link disabled" tabindex="-1" data-publisher="American Chemical Society"><span class="link__text text-meta text-bold text-italic">Inorganic Chemistry</span><span class="sr-only">this link is disabled</span></a>,
<span class="text-meta">2022, 61(3), pp. 1685–1696</span></div><els-collapsible-panel-v2 open="false" data-testid="document-abstract-link" data-component="document-abstract-link" control-label="Show abstract"
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<div class="text-width-38">The generation of pure H2 from a neutral electrolyte solution represents a transformative route with low cost and environmentally friendly nature. However, the complex kinetics of
hydrogen evolution reaction (HER) via water electrolysis make its practical application to be difficult. Herein, we have reported Ru-doping-induced formation of VS4 nanostructures with a rich S vacancy
for neutral HER in a 0.2 M phosphate buffer solution. The Ru-doped VS4 demands an overpotential value of 160 mV at 10 mA/cm2 current density with a lower catalyst loading of 0.1 mg/cm2, while pristine VS4
demands a 374 mV overpotential with the same mass loading. 60 hours of chronoamperometric study reveals the excellent stability of Ru-doped VS4 materials, which is the highest amount of time ever reported
for neutral HER. The marginal degradation of a catalyst under a long-term stability study was confirmed through inductively coupled plasma mass spectrometry (ICP-MS) analysis. The introduction of Ru to
the VS4 lattice leads to a 4.35-fold increase in the turnover-frequency values compared to those of bare VS4 nanostructures. The higher HER activity of S-vacancy-enriched VS4 materials is thought to
originate through effective water adsorption in S vacancy and Ru3+ sites followed by the dissociation of a H2O molecule, and S22- efficiently converts Had to H2. Also, post-HER characterization reveals
that the transformation of some Ru3+ to Ru0 additionally favored the HER by providing a better H adsorption site under a static cathodic potential.</div>
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EL-BAHY, ZEINHOM MOHAMED A.
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Al-Azhar Universitydisabled, Nasr City, Egypt
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RESULTS LIST, SHOWING RESULTS 1 THROUGH 10 OF 62 RESULTS.
* Article
Electronic structure, optical, thermoelectric and magnetic properties of
A2CdP2 (A = Ca, Sr and Ba) n-type narrow band gap semiconductors
Aman, S., Albalawi, H., Tahir Farid, H.M., Mahmoud, K.H., El-Bahy, Z.M.
Materials Science in Semiconductor Processingthis link is disabled, 2022,
142, 106443
Show abstract
Related documents
Structural, Optoelectronic, thermoelectric and magnetic properties of A2CdP2
(A = Ca, Sr and Ba) Zentl phase compounds in Cmc21 symmetry are investigated
using FP-LAPW method with GGA-PBE, GGA-PBEsol, HSE06, G0W0 and GGA-mBJ
potentials based on DFT. Estimated structure parameters are well agreement
with the experiment. Cohesive energy shows that Ba2CdP2 is more stale then
the rest compounds and posses high melting point. Electronic properties shows
that all the compounds are direct band gap semiconductors at central symmetry
while GGA-mBJ transit the direct band gap nature to indirect nature at ᴦ-H
symmetry. The direct band gap values are ranging from 0.74 to 1.47 eV. The
calculated band gaps are decreasing with the cation replacement and
increasing by hybrid functionals. The result revel that all the compounds are
optically active in infrared region of electromagnetic spectrum. Optical
properties reveals that these compounds can be used as potential candidate
for optoelectronic devices. Due to the narrow band gap semiconducting nature
of these compounds their thermoelectric parameters are also calculated which
shows that these compounds are efficient to use as the active thermoelectric
materials. DFT and Post-DFT calculation indicate the paramagnetic nature of
all compounds.
0
Citations
* Article
Highly dispersed active sites of Ni nanoparticles onto hierarchical reduced
graphene oxide architecture towards efficient water oxidation
Zeenat, Maryum Javed, S., Ahmad, Z., ...Elnaggar, A.Y., El-Bahy, Z.M.
Fuelthis link is disabled, 2022, 312, 122926
Show abstract
Related documents
Herein, we reported a facile route to fabricate the Ni-NPs decorated over
reduced graphene oxide (Ni/rGO) nanocomposite by an in-situ reduction method.
It has been observed that the Ni/rGO drived the water oxidation at a very low
overpotential of 1.42 VRHE (ŋ = 190 mV). Furthermore, the robust catalyst
presented an extraordinary porosity and imperious kinetics performance while
showing a high time of flight (0.2 s−1), mass activity (28 A/g) and smaller
value of Tafel slope (62 mVdec−1) at an applied potential of 0.35 VRHE only.
Ni/rGO also exhibited stable current density which leftovers sustained in
alkaline water catalysis conducted for a prolonged time without any
significant loss in catalytic efficiency. This outstanding catalytic activity
of hierarchical Ni/rGO is comparable to avant-garde electrocatalytic material
and even much better than the noble and transitional metal-centred
eensy-weensy electrocatalytic assemblies with several drawbacks.
1
Citations
* Article
DFT study of OLi3 and MgF3 doped boron nitride with enhanced nonlinear
optical behavior
Shafiq, S., Shehzad, R.A., Yaseen, M., ...Mahmoud, K.H., El-Bahy, Z.M.
Journal of Molecular Structurethis link is disabled, 2022, 1251, 131934
Show abstract
Related documents
The electrical and optical properties of superalkali (OLi3) and superhalogen
(MgF3) doped boron nitride nanocage are investigated. Superalkali and
superhalogen are doped physically and substitutionally with boron nitride and
its geometrical and optoelectronic properties are analyzed and compared
systematically. In the doped nanocage of boron nitride, the linear optical
polarizability and nonlinear optical hyperpolarizability increases to a
greater extent. The increasing trend of the hyperpolarizability in the
nanocage of metal-doped boron nitride depends on the atomicity of
superhalogen and superalkali metal. The energy bandgap of HOMO-LUMO also
decreases due to the injection of new energy levels in all the doped
compounds of boron nitride near the Fermi level. Among different
combinations, MgF3 and OLi3 doped with B12N10 found the most reliable
combination with enhanced linear and nonlinear optical polarizability. The
current clue gives wide applications for boron nitride nanocage in electrical
instruments and devices that play an important role in the designing of
efficient nonlinear optical materials.
1
Citations
* Article
Synthesis, In silico and in vitro studies of Silver (I)-N heterocyclic
carbene complexes
Sarfraz, A., Ashraf, R., Ali, S., ...El-Bahy, S.M., El-Bahy, Z.M.
Journal of Molecular Structurethis link is disabled, 2022, 1251, 131946
Show abstract
Related documents
In the present study, four silver based NHC (N-heterocyclic carbene)
complexes (1c-4c) were designed and synthesized from their precursor salts
(1b-4b). The successful synthesis of salts and complexes was assured through
spectroscopic techniques (UV-visible, FTIR, 1H NMR) as well as mass
spectrometry. The in silico ADMET study and molecular docking calculations
predicted the compounds are good drug candidates having therapeutic potential
against multiple cancer targets including COX-1, VEGFA, HIF as well as VGF.
Results of in vitro study conducted through MTT assay confirmed that all test
compounds have concentration dependent potency but silver complexes (1c-4c)
have far superior activity than precursor, salts (1b-4b) and slightly lower
than standard drugs (carboplatin and cisplatin) against various cancer cell
lines. Among the studied compounds, 3c showed lowest IC50 value of 0.981 ±
0.09, 1.10 ± 0.14 and 0.973 ± 0.12 µg/mL against MCF-7, HCT-116 and A549
respectively. The test compounds were found good antibacterial agents, when
screened against bacterial strains (Staphylococcus aureus, Micrococcus
luteus, Escherichia coli and S. typhimurium), as well as antioxidant agents
when tested against DPPH free radicals.
0
Citations
* Article
SAPO-34 crystallized using novel pyridinium template as highly active
catalyst for synthesis of ethyl levulinate biofuel
Ma, Y.-K., Chia, S., Daou, T.J., ...Ling, T.C., Ng, E.-P.
Microporous and Mesoporous Materialsthis link is disabled, 2022, 333, 111754
Show abstract
Related documents
Silicoaluminophosphate Number 34 (SAPO-34) crystallized using novel
N-heterocyclic organic template—1-propylpyridinium hydroxide ([PPy]OH)—as an
excellent catalyst for the production of ethyl levulinate biofuel is
reported. First, the time-dependent crystallization study of SAPO-34 using
various spectroscopy, microscopy and analytical techniques is performed and
it reveals that the precursor undergoes several important crystallization
steps, namely dissolution of reactants (induction), nucleation and crystal
growth of SAPO-34, before it transforms into a more metastable SAPO-36
crystalline phase. The resulting SAPO-34 solid (Si0.198Al0.475P0.327O2)
exhibits high porosity (SBET = 673 m2/g, VTot = 0.27 cm3/g) and high Si
content (Si/(Si + Al + P) = 0.198) which contribute to high surface acidity
(2.52 mmol/g) as confirmed by the NH3-TPD analysis. The SAPO-34 catalyst
shows 93.4% conversion to ethyl levulinate via esterification of levulinic
acid with ethanol just within 20 min at 190 °C under non-microwave instant
heating, which is considered very fast as compared to other systems. In
addition, high catalyst recyclability is observed even after fifth cycle of
reaction, thus offering another promising pathway for crystallizing zeolites
using this new class of template that are beneficial for catalytic biofuel
upgrading process.
0
Citations
* Article • Open access
ZIF-8-derived ZnO/C decorated hydroxyl-functionalized multi-walled carbon
nanotubes as a new composite electrode for supercapacitor application
Otun, K.O., Xaba, M.S., Zong, S., ...Alotaibi, M.T., El-Bahy, Z.M.
Colloids and Interface Science Communications, 2022, 47, 100589
Show abstract
Related documents
Due to the poor conductivity of metal-organic frameworks (MOFs), it is
challenging to directly employ MOFs as electrode materials for
supercapacitors. Herein, hydroxyl-functionalized multi-walled carbon nanotube
(f-MWCNT) was used to decorate ZnO/C obtained from the prior calcination of
pristine zeolitic imidazolate framework-8 (ZIF-8) and applied as electrode
material for supercapacitor application. The resulting ZnO/C@f-MWCNT
electrode exhibits excellent storage performance, as confirmed by the
specific capacitance of 650 F/g at 1 A/g and a superior energy/power density
compared to the single electrode. Additionally, the composite electrode
displayed remarkable cycling stability of 70% after 5000 cycles and retained
75% of its initial capacitance at 10 A/g, demonstrating good rate
cyclability. The exceptional performance of ZnO/C@f-MWCNT was attributed to
the synergistic effects offered by f-MWCNT which improved its electrical
conductivity and ZnO/C that provided sufficient redox-active sites and
structural stability. This work may promote the design of advanced MOF-based
nanocomposites for energy storage application.
0
Citations
* Article
A n-butanol gas sensor with enhanced gas sensing performance based on
Co-doped BiVO4 polyhedrons
Guo, W., Shuai, Y., Liu, X., ...El-Bahy, Z.M., Mubarak, N.M.
Sensors and Actuators B: Chemicalthis link is disabled, 2022, 354, 131221
Show abstract
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N-butanol, a poisonous and flammable liquid, has great threat to human life
and property security, which is of importance to monitor n-butanol in the
environment. In this paper, the pure and Co-doped BiVO4 polyhedrons are
successfully synthesized by hydrothermal method. A series of
characterizations, such as XRD, XPS, SEM, UV, and EIS, etc., are used to
analyze the crystal structure, morphology, element compositions, optical and
electrochemical properties of the as-prepared samples. The optimal sample
(3Co-BiVO4) exhibits high gas response (51.65) toward 100 ppm n-butanol,
which is around four times higher than that of pure BiVO4 at 300 °C. In
addition, the 3Co-BiVO4 also has fast response-recovery time, good humidity
resistance, favorable selectivity to n-butanol, etc. Based on the above
characterizations and gas sensing test results, the enhanced gas sensing
mechanism for 3Co-BiVO4 is proposed. This work provides a feasible strategy
to fabricate BiVO4 polyhedron by doping Co to greatly enhance the gas sensing
properties for n-butanol.
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Citations
* Article
Biodiesel synthesis from Prunus bokhariensis non-edible seed oil by using
green silver oxide nanocatalyst
Dawood, S., Ahmad, M., Zafar, M., ...El-Bahy, Z.M., Khoo, K.S.
Chemospherethis link is disabled, 2022, 291, 132780
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The present work investigates the proficiency of green silver oxide
nanocatalyst synthesised from Monotheca buxifolia (Falc.) Dcne. leaves
extract, and their application for biodiesel synthesis from novel Prunus
bokhariensis seed oil (non-edible). The seed oil content of 55% and FFA
content of 0.80 mg KOH/g were reported. Several analytical tools (EDX, FT-IR,
SEM and XRD) were used to characterise the Ag2O nanocatalyst. Maximum (89%)
FAME yield of the PBSOB (Prunus bokhariensis seed oil biodiesel) was achieved
at ambient transesterification conditions i.e. 3.5 wt% nanocatalyst loading,
2.5 h reaction time, 130 °C of reaction temperature and 12:1 alcohol to oil
ratio. The synthesised PBSOB was additionally characterised by analytical
methods like, GC-MS and FT-IR. The different aspects of fuel were identified
i.e. flash point (84 °C), kinematic viscosity (4.01 cSt @ 40 °C), sulphur
content (0.0003 wt %), density (0.853 kg/L) and acid number (0.167 mg KOH/g).
All the above properties were verified and agreed well with biodiesel
international standards (European Union (14214), China GB/T (20828) and ASTM
(6751, 951). In general, Prunus bokhariensis seed oil and Ag2O nanocatalyst
seem to be remarkably active, cheap and stable candidates for the biodiesel
industry in future.
1
Citations
* Article
Double linker MOF-derived NiO and NiO/Ni supercapacitor electrodes for
enhanced energy storage
Otun, K.O., Xaba, M.S., Zong, S., ...El-Bahy, S.M., El-Bahy, Z.M.
Colloids and Surfaces A: Physicochemical and Engineering Aspectsthis link is
disabled, 2022, 634, 128019
Show abstract
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Metal-organic frameworks (MOFs)-derived nanomaterials have emerged as novel
electrodes for electrochemical energy storage application. Herein,
MOF-derived NiO and NiO/Ni composite electrodes have been successfully
synthesized by a unique double-linker MOF-strategy involving a series of
calcination procedures (400 °C, 500 °C and 600 °C). The introduction of
calcination temperature influenced both the textural and electrochemical
properties of the MOF-derived NiO/Ni-400 and NiO/Ni-500 composite electrodes
obtained at 400 °C and 500 °C respectively, as well as the NiO-600 electrode
produced at 600 °C. With the combined benefits of improved uniform pore-size
distribution and electrical conductivity, the composite electrodes delivered
an enhanced supercapacitor performance with specific capacitances of 104.6
mAg−1 (NiO/Ni-400) and 37.4 mAg−1 (NiO/Ni-500) compared with 28.5 mAg−1 for
the NiO-600 electrode at the same current density. Interestingly, NiO/Ni
retained about 90% of its original capacitance after 1000 cycles when
measured in 3 M KOH electrolyte solution. Furthermore, the electrochemical
kinetic analysis used to probe the energy storage mechanism revealed
pseudocapacitive behaviors at all tested scan rates; with NiO/Ni contributing
67% of the total capacitance at a scan rate of 5 mV/s which increased to 87%
at 100 mV/s. The results obtained confirm that the approach described in this
study is promising for the design of MOF-based electrodes for energy storage
applications.
1
Citations
* Article
Ruthenium-Doping-Induced Amorphization of VS4Nanostructures with a Rich
Sulfur Vacancy for Enhanced Hydrogen Evolution Reaction in a Neutral
Electrolyte Medium
Karmakar, A., Sankar, S.S., Kumaravel, S., ...El-Bahy, Z.M., Kundu, S.
Inorganic Chemistrythis link is disabled, 2022, 61(3), pp. 1685–1696
Show abstract
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The generation of pure H2 from a neutral electrolyte solution represents a
transformative route with low cost and environmentally friendly nature.
However, the complex kinetics of hydrogen evolution reaction (HER) via water
electrolysis make its practical application to be difficult. Herein, we have
reported Ru-doping-induced formation of VS4 nanostructures with a rich S
vacancy for neutral HER in a 0.2 M phosphate buffer solution. The Ru-doped
VS4 demands an overpotential value of 160 mV at 10 mA/cm2 current density
with a lower catalyst loading of 0.1 mg/cm2, while pristine VS4 demands a 374
mV overpotential with the same mass loading. 60 hours of chronoamperometric
study reveals the excellent stability of Ru-doped VS4 materials, which is the
highest amount of time ever reported for neutral HER. The marginal
degradation of a catalyst under a long-term stability study was confirmed
through inductively coupled plasma mass spectrometry (ICP-MS) analysis. The
introduction of Ru to the VS4 lattice leads to a 4.35-fold increase in the
turnover-frequency values compared to those of bare VS4 nanostructures. The
higher HER activity of S-vacancy-enriched VS4 materials is thought to
originate through effective water adsorption in S vacancy and Ru3+ sites
followed by the dissociation of a H2O molecule, and S22- efficiently converts
Had to H2. Also, post-HER characterization reveals that the transformation of
some Ru3+ to Ru0 additionally favored the HER by providing a better H
adsorption site under a static cathodic potential.
0
Citations
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